pinto
High pressure reactor pinto
Our high-pressure autoclave "pinto" combines the technology and know-how of a pneumatic professional model, but it features a fundamentally different chassis. A 4-sided tubular frame in chrome steel provides maximum ground clearance for the drain valve or collection vessel and, in addition, the cooling water valve is easily accessible.
Specifications
- Nominal volume ml: 500, 1000
- Working pressure in bar: 200, 250
- Working temperature °C: 200
- Material WNr. 1.4435 or WNr. 2.4602
- Jaw closure (quick release)
- Viton O-ring lying in autoclave vessel
- Magnetic stirrer drive funrun in combination with three-phase motor 120W
- Torque of magnetic coupling 60 Ncm, respectively 90 Ncm
- Output speed with ball bearing 0-1'300 rpm, with plain bearing 0-1'200 rpm.
- Pressure station on the chassis with manometer and pressure transducer 0-250 bar
- Needle valve for gas supply
- Needle valve for pressure relief
- Needle valve with dip tube for sampling and emptying
- Bursting disc holder equipped with bursting disc 250 bar
- Immersion tube with temperature sensor type K or Pt100 4p for fluid heating version
- Stirring element: diagonal blade stirrer
- Electric heating or fluid heating
Variants/special features
Versions vary for the standard versions
- From 200 bar we use expansion bolts and nuts.
- Viton or other O-ring qualities on request
- Magnetic stirrer drive funrun in combination with three-phase motor 120W or a Heidolph drive
- With the magnetic stirrer funrun the three-phase motor is directly flange-mounted, the Heidolph drive, on the other hand, is connected via a flexible coupling (macline magnetic stirrer system).
- Output speed with ball bearing 0-1'300 rpm, with plain bearing 0-1'200 rpm.
- Heating: electric heating and fluid heating via heat transfer oil
- Immersion tube with temperature sensor type K for electric heating and Pt100 4p for fluid heating version
- Stirring element: diagonal blade stirrer
Special equipment according to model for the production of nanoparticles
- Nominal volume 400 ml and glass liner
- 220 bar and 300°C working conditions, WNr. 2.4602 for wetted parts
- All welded parts electropolished
- Closure: expansion screws and nuts
- Seal: silver ring
- Pressure part of magnetic stirrer with cooling zone
- Plain bearing graphite 1-1'200 rpm.
- Armature and helix stirrer in HC22
- Immersion tube HC22 with thermosensor type K
- Fittings of the pressure station protected by a central diaphragm
- Viewing window and connection for PH probe
- Sitec valve SS with connecting pipes in HC22
- Bottom outlet valve
Production of nanocoatings
The reactor shown is used for the synthesis of nanoparticles by hydrathermal synthesis. This means that the substances are crystallised from aqueous high-temperature solutions at high steam pressures. The optical cells used in the autoclave are used to monitor the reactions using UV-VIS or RAMAN spectrometry. The nanoparticles are used to develop nanocoatings for glass of buildings, cars, solar panels and others. The function of the nanocoating can be diverse, such as reflecting thermal radiation, glare-free vision, privacy protection, temperature barrier on the surface.
| Article No | Vol. ml | Pres PS bar | Temp. TS C° | Pres PA bar | Temp. PA C° | Mat. WNr. | Sensor / Heating | Drive / Version | L x W x H mm |
|---|---|---|---|---|---|---|---|---|---|
| 134125 | 500 | 250 | 300 | 200 | 200 | 1.4435 | Type K, electric | 60 Ncm/Motor 120W | 611x540x1160 |
| 134164 | 500 | 250 | 300 | 200 | 200 | 2.4602 | Type K, electric | 60 Ncm/Motor 120W | 611x540x1160 |
| 134200 | 500 | 250 | 300 | 200 | 200 | 1.4435 | 1 x Pt100, fluid | Heidolph drive | 611x540x1356 |
| 134355 | 500 | 250 | 300 | 200 | 200 | 2.4602 | 1 x Pt100, fluid | Heidolph drive | 611x540x1356 |
| 134111 | 1000 | 250 | 300 | 200 | 200 | 1.4435 | Type K, electric | 90 Ncm/Motor 180W | 611x540x1197 |
| 134166 | 1000 | 250 | 300 | 200 | 200 | 2.4602 | Type K, electric | 90 Ncm/Motor 180W | 611x540x1197 |
| 134360 | 1000 | 250 | 300 | 200 | 200 | 1.4435 | 1 x Pt100, fluid | Heidolph drive | 611x540x1356 |
| 134367 | 1000 | 250 | 300 | 200 | 200 | 2.4602 | 1 x Pt100, fluid | Heidolph drive | 611x540x1356 |
